LeHavreV1, France, Analysis, bibRecord, 001361

Synthesis of thieno[2′,3′(3′,4′ or 3′,2′):5,6]azepino[2,1‐a]isoindolediones from N‐Thienyl‐2(3)‐ylmethylphthalimides

Identifieur interne : 001361 ( France/Analysis ); précédent : 001360; suivant : 001362

Synthesis of thieno[2′,3′(3′,4′ or 3′,2′):5,6]azepino[2,1‐a]isoindolediones from N‐Thienyl‐2(3)‐ylmethylphthalimides

Auteurs : Pascal Pigeon [France] ; Bernard Decroix [France]

Source :

Journal of Heterocyclic Chemistry [ 0022-152X ] ; 1996-01.

RBID : ISTEX:6E945CAECF0C8D1D4BE4D004CC0B6FBD8AD81B26

Abstract

Reduction of N‐thienybnethylphthalimides 5a‐e followed by the Wittig reaction gave the substituted acetic acids 8a‐e. Their corresponding acyl chlorides where cyclized in the presence of aluminium trichloride to furnish the cyclic ketones 9a‐e. Treatment of these ketones with bromine followed by triethylamine, or with selenium dioxide led to the thienoazepinoisoindolediones 1a‐e.

Url:

https://api.istex.fr/document/6E945CAECF0C8D1D4BE4D004CC0B6FBD8AD81B26/fulltext/pdf

DOI: 10.1002/jhet.5570330123

Affiliations:

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to stream Istex, to step Curation: 000129
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to stream Main, to step Curation: 001F19
to stream Main, to step Exploration: 001F19
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ISTEX:6E945CAECF0C8D1D4BE4D004CC0B6FBD8AD81B26

Le document en format XML

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<author><name sortKey="Pigeon, Pascal" sort="Pigeon, Pascal" uniqKey="Pigeon P" first="Pascal" last="Pigeon">Pascal Pigeon</name>
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<author><name sortKey="Decroix, Bernard" sort="Decroix, Bernard" uniqKey="Decroix B" first="Bernard" last="Decroix">Bernard Decroix</name>
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<front><div type="abstract">Reduction of N‐thienybnethylphthalimides 5a‐e followed by the Wittig reaction gave the substituted acetic acids 8a‐e. Their corresponding acyl chlorides where cyclized in the presence of aluminium trichloride to furnish the cyclic ketones 9a‐e. Treatment of these ketones with bromine followed by triethylamine, or with selenium dioxide led to the thienoazepinoisoindolediones 1a‐e.</div>
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Synthesis of thieno[2′,3′(3′,4′ or 3′,2′):5,6]azepino[2,1‐a]isoindolediones from N‐Thienyl‐2(3)‐ylmethylphthalimides

Synthesis of thieno[2′,3′(3′,4′ or 3′,2′):5,6]azepino[2,1‐a]isoindolediones from N‐Thienyl‐2(3)‐ylmethylphthalimides

Source :

Abstract

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Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri